The ITDD Purification and Analytical Services Facility carries out a variety of small-molecule analyses and purifications on a regular basis including LC-MS, low resolution mass spectrometry (LRMS), preparative, reverse phase liquid chromatography, and NMR. These analyses are facilitated by on-site instruments that include a Waters UPLC, two Waters ZQ mass spectrometers, a Waters autopurification system, and a Bruker 400 MHz NMR spectrometer.
Services
Services
- Low-resolution mass spectrometry
- UPLC-MS
- Reverse-phase, preparative separations
- NMR experiments (1H, 13C, others)
- Compound plating and dispensing
- Vial weighing
Additional Analytical Equipment
- Autopol V Polarimeter
- Perkin-Elmer IR Spectrophotometer
- 785 Karl Fisher Titrino System
Core Capabilities
- 400 MHz Bruker NMR
- Autopol V Polarimeter
- Waters Acquity uPLC with ZQ mass spectrometer
- Waters Autopurification system with ZQ mass spectrometer
- Perkin-Elmer IR Spectrophotometer
- Waters Preparative and Analytical HPLC
- 785 Karl Fischer Titrino System
Contact
Shameem Sultana Syeda, Ph.D.
Director, Lead and Probe Discovery Core
Telephone: 612-626-6864
Email: [email protected]